[리포트] Beckmann rearrangement
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작성일 19-05-24 07:13
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Download : [레포트] Beckmann rearrangement.hwp
-Reaction mechanism
5. Material
(1) Reagent
-Hydroxylamine hydrochloride
Chemical formula:
Molar mass: 69.49 g/mol
Appearance: white crystalline solid
Density: 1.67 g/cm³
Melting point: 155 to 157 °C
monoclinic columnar crystal. water 1mL, alcohol 19mL, methanol 8mL에 1g 녹음. glycerol, propylene glycol에 soluble. 차가운 ether에 insoluble. 잘 닫아서 보관해야 한다.
주의: skin irritant.
-Water(hydrogen oxide)
Molecular formula:
Molar mass: 18.01528 g/mol
Appearance: white solid or almost colorless, transparent, with a slight hint of blue, crystalline solid or liquid
Density: 1000 kg/m³ = 1 g/cm³ liquid (maximum, at about 4 °C) 91…(생략(省略))
[레포트] Beckmann rearrangement , [레포트] Beckmann rearrangement공학기술레포트 , 레포트 Beckmann rearrangement
[리포트] Beckmann rearrangement
레포트/공학기술
![[레포트]%20Beckmann%20rearrangement_hwp_01.gif](http://www.allreport.co.kr/View/%5B%EB%A0%88%ED%8F%AC%ED%8A%B8%5D%20Beckmann%20rearrangement_hwp_01.gif)
![[레포트]%20Beckmann%20rearrangement_hwp_02.gif](http://www.allreport.co.kr/View/%5B%EB%A0%88%ED%8F%AC%ED%8A%B8%5D%20Beckmann%20rearrangement_hwp_02.gif)
![[레포트]%20Beckmann%20rearrangement_hwp_03.gif](http://www.allreport.co.kr/View/%5B%EB%A0%88%ED%8F%AC%ED%8A%B8%5D%20Beckmann%20rearrangement_hwp_03.gif)
![[레포트]%20Beckmann%20rearrangement_hwp_04.gif](http://www.allreport.co.kr/View/%5B%EB%A0%88%ED%8F%AC%ED%8A%B8%5D%20Beckmann%20rearrangement_hwp_04.gif)
![[레포트]%20Beckmann%20rearrangement_hwp_05.gif](http://www.allreport.co.kr/View/%5B%EB%A0%88%ED%8F%AC%ED%8A%B8%5D%20Beckmann%20rearrangement_hwp_05.gif)
![[레포트]%20Beckmann%20rearrangement_hwp_06.gif](http://www.allreport.co.kr/View/%5B%EB%A0%88%ED%8F%AC%ED%8A%B8%5D%20Beckmann%20rearrangement_hwp_06.gif)
순서
Download : [레포트] Beckmann rearrangement.hwp( 44 )
다.레포트,Beckmann,rearrangement,공학기술,레포트
[리포트] Beckmann rearrangement
설명
1. Subject : Beckmann rearrangement
2. Date :
3. Name :
4. Principle
-Beckmann rearrangement는 oxime을 amide로 바꿔주는 reaction response이다. carbonyl compound에서 imine을 생성할 때, intermediate로 oxime이 되게 만들어준다면 amide를 쉽게 생성할 수 있따
-이번 實驗에서는 cyclohexannone를 reactant로 하여, cyclohecaneone oxime을 reaction intermediate로 형성하였다가 beckmann rearrangement를 통해 caprolactam을 얻는다.
